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x ray diffraction patterns  (Rigaku Corporation)
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Physicochemical and mechanical characterization of the hydrogel formulations. A) Schematic illustration of the preparation of GA–Zn 2+ /BP@SilMA and incorporation of osteogenic bone microtissues (BO). B) Photographs of the hydrogel precursor before and after ultraviolet. C) Scanning electron microscopy (SEM) images of SilMA, GA–Zn 2+ @SilMA, GA–Zn 2+ /BP@SilMA, and GA–Zn 2+ /BP/BO@SilMA hydrogels. D) <t>Energy-dispersive</t> <t>X-ray</t> spectroscopy (EDS) elemental maps of C, O, P, and Zn in the composite hydrogel. E) Fourier-transform infrared spectroscopy (FTIR) spectra of the different hydrogel formulations. F) X-ray <t>diffraction</t> (XRD) patterns of the different hydrogel formulations. G) Atomic force microscopy (AFM) force–separation curves. H) Zn 2+ release profile. I) Degradation behavior of the hydrogel. J) Young's modulus of the different hydrogel formulations. Data are presented as mean ± SD. *p < 0.05 and ****p < 0.0001.
X Ray Diffraction Patterns, supplied by Rigaku Corporation, used in various techniques. Bioz Stars score: 99/100, based on 1 PubMed citations. ZERO BIAS - scores, article reviews, protocol conditions and more
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Solid‐state characterization of L ‐TASe and D ‐TASe crystals. (a) Experimental <t>PXRD</t> patterns of L ‐TASe and D ‐TASe and simulated pattern from SCXRD data, confirming phase purity and crystallinity. (b) FTIR spectra of L ‐TASe and D ‐TASe , showing amide I and amide II vibrations. (c) Solid‐state CD and absorption spectra of L ‐TASe and D ‐TASe . Mirror‐image Cotton effects confirm their enantiomeric relationship. (d) TGA curves of L ‐TASe and D ‐TASe , showing thermal stability up to 290°C. (e) <t>PXRD</t> patterns of L ‐TASe after 30‐day immersion in aqueous media at pH 2.0 – 7.8, demonstrating chemical robustness. (f) CO 2 adsorption‐desorption isotherms of L ‐TASe at 273 K. Inset: pore size distribution, revealing microporous features.
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Physicochemical and mechanical characterization of the hydrogel formulations. A) Schematic illustration of the preparation of GA–Zn 2+ /BP@SilMA and incorporation of osteogenic bone microtissues (BO). B) Photographs of the hydrogel precursor before and after ultraviolet. C) Scanning electron microscopy (SEM) images of SilMA, GA–Zn 2+ @SilMA, GA–Zn 2+ /BP@SilMA, and GA–Zn 2+ /BP/BO@SilMA hydrogels. D) Energy-dispersive X-ray spectroscopy (EDS) elemental maps of C, O, P, and Zn in the composite hydrogel. E) Fourier-transform infrared spectroscopy (FTIR) spectra of the different hydrogel formulations. F) X-ray diffraction (XRD) patterns of the different hydrogel formulations. G) Atomic force microscopy (AFM) force–separation curves. H) Zn 2+ release profile. I) Degradation behavior of the hydrogel. J) Young's modulus of the different hydrogel formulations. Data are presented as mean ± SD. *p < 0.05 and ****p < 0.0001.

Journal: Materials Today Bio

Article Title: Hydrogel-integrated osteogenic microtissues promote repair of infected intervertebral defects through sequential immunomodulation

doi: 10.1016/j.mtbio.2026.103657

Figure Lengend Snippet: Physicochemical and mechanical characterization of the hydrogel formulations. A) Schematic illustration of the preparation of GA–Zn 2+ /BP@SilMA and incorporation of osteogenic bone microtissues (BO). B) Photographs of the hydrogel precursor before and after ultraviolet. C) Scanning electron microscopy (SEM) images of SilMA, GA–Zn 2+ @SilMA, GA–Zn 2+ /BP@SilMA, and GA–Zn 2+ /BP/BO@SilMA hydrogels. D) Energy-dispersive X-ray spectroscopy (EDS) elemental maps of C, O, P, and Zn in the composite hydrogel. E) Fourier-transform infrared spectroscopy (FTIR) spectra of the different hydrogel formulations. F) X-ray diffraction (XRD) patterns of the different hydrogel formulations. G) Atomic force microscopy (AFM) force–separation curves. H) Zn 2+ release profile. I) Degradation behavior of the hydrogel. J) Young's modulus of the different hydrogel formulations. Data are presented as mean ± SD. *p < 0.05 and ****p < 0.0001.

Article Snippet: Energy-dispersive X-ray spectroscopy (EDS, Sigma 360, ZEISS, Germany) mapping was used to examine the distribution of C, O, Zn, and P.Fourier transform infrared spectroscopy(FTIR, Nicolet iS50, Thermo Fisher Scientific, USA) was performed with 32 scans in the range of 4000–400 cm −1 at a resolution of 4 cm −1 ; X-ray diffraction patterns (XRD, SmartLab SE, Rigaku Corporation, Japan) were recorded from 5° to 90°.

Techniques: Scanning Electron Microscopy, Energy Dispersive X-Ray, Spectroscopy, Fourier Transform Infrared Spectroscopy, Microscopy

Solid‐state characterization of L ‐TASe and D ‐TASe crystals. (a) Experimental PXRD patterns of L ‐TASe and D ‐TASe and simulated pattern from SCXRD data, confirming phase purity and crystallinity. (b) FTIR spectra of L ‐TASe and D ‐TASe , showing amide I and amide II vibrations. (c) Solid‐state CD and absorption spectra of L ‐TASe and D ‐TASe . Mirror‐image Cotton effects confirm their enantiomeric relationship. (d) TGA curves of L ‐TASe and D ‐TASe , showing thermal stability up to 290°C. (e) PXRD patterns of L ‐TASe after 30‐day immersion in aqueous media at pH 2.0 – 7.8, demonstrating chemical robustness. (f) CO 2 adsorption‐desorption isotherms of L ‐TASe at 273 K. Inset: pore size distribution, revealing microporous features.

Journal: Advanced Science

Article Title: Supramolecular Chiral Assemblies from Benzoselenadiazole‐Alanine‐Acylhydrazone Conjugates Enable Cardioprotection

doi: 10.1002/advs.77953

Figure Lengend Snippet: Solid‐state characterization of L ‐TASe and D ‐TASe crystals. (a) Experimental PXRD patterns of L ‐TASe and D ‐TASe and simulated pattern from SCXRD data, confirming phase purity and crystallinity. (b) FTIR spectra of L ‐TASe and D ‐TASe , showing amide I and amide II vibrations. (c) Solid‐state CD and absorption spectra of L ‐TASe and D ‐TASe . Mirror‐image Cotton effects confirm their enantiomeric relationship. (d) TGA curves of L ‐TASe and D ‐TASe , showing thermal stability up to 290°C. (e) PXRD patterns of L ‐TASe after 30‐day immersion in aqueous media at pH 2.0 – 7.8, demonstrating chemical robustness. (f) CO 2 adsorption‐desorption isotherms of L ‐TASe at 273 K. Inset: pore size distribution, revealing microporous features.

Article Snippet: Powder x‐ray diffraction (PXRD) patterns were recorded on a SmartLab diffractometer, Rigaku, Japan, using Cu Kα radiation at room temperature with a step size of 0.02°.

Techniques: Stability, Adsorption, Pore Size